Citation: Yunhan Gao, Xing Sun, Mengxia Ji, Xingchang Qiu, Tiange Wei, Qing Xu, Sheng Yin, Jiexiang Xia, Huaming Li. Hierarchical ZIF-derived carbon/Bi₁₂O₁₇Cl₂ heterostructures synergistically enhance electron dynamics and optical properties to boost CO₂ photoreduction in pure water[J]. Acta Physico-Chimica Sinica, ;2026, 42(10): 100264. doi: 10.1016/j.actphy.2026.100264 shu

Hierarchical ZIF-derived carbon/Bi₁₂O₁₇Cl₂ heterostructures synergistically enhance electron dynamics and optical properties to boost CO₂ photoreduction in pure water

Yunhan Gao ¹ ,
Xing Sun ² ,
Mengxia Ji ^1,, ,
Xingchang Qiu ¹ ,
Tiange Wei ¹ ,
Qing Xu ² ,
Sheng Yin ² ,
Jiexiang Xia ^2,, ,
Huaming Li ^1,,

1.
Institute for Energy Research, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China;
2.
School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China

Corresponding author: Mengxia Ji, Jiexiang Xia, Huaming Li,
Received Date: 3 December 2025
Revised Date: 16 February 2026
Accepted Date: 25 February 2026

Conventional Bi₁₂O₁₇Cl₂ photocatalyst suffer from narrow solar harvesting, weak CO₂ adsorption and poor charge utilization. Herein, an intimate hierarchical heterojunction was constructed by embedding Bi₁₂O₁₇Cl₂ ultrathin nanotubes into hierarchical Co-ZIF-derived porous carbon (Co-PC/BOC). Multi-cavity reflection within Co-PC nanocages and localized surface plasmon resonance of in situ generated Co₃O₄ domains synergistically enhance the light harvest ability of the Co-PC/BOC in the full spectral range. In pure water without any photosensitizers or sacrificial agents, the optimal composite exhibits a CO yield of 34.16 μmol g^-1 h^-1 with 100% selectivity, 2.9-fold higher than bare BOC. In situ DRIFTS and photo/electrochemical characterizations demonstrate that Co-PC serves as a dual-function platform of plasmonic hot-electron injector and charge separation hub, whereas BOC provide abundant surface sites for *COOH formation and *CO cleavage. Our work highlights the promising potential of metal-organic frameworks and their derivatives in developing efficient artificial photosynthesis systems.
- Bi₁₂O₁₇Cl₂ nanotube,
- MOFs derivative,
- Charge separation,
- Plasmon resonance,
- CO₂ photoreduction
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Hierarchical ZIF-derived carbon/Bi12O17Cl2 heterostructures synergistically enhance electron dynamics and optical properties to boost CO2 photoreduction in pure water

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通讯作者: 陈斌, bchen63@163.com

Hierarchical ZIF-derived carbon/Bi₁₂O₁₇Cl₂ heterostructures synergistically enhance electron dynamics and optical properties to boost CO₂ photoreduction in pure water