Citation: Yuge Fan, Xianliang Fu, Li Zhu, Man Xu. Small changes, big differences: modified KSCN molten salt method for one-pot synthesis of Cd vacancy-enriched MoS₂/CdS and the enhanced photocatalytic H₂ evolution performance[J]. Acta Physico-Chimica Sinica, ;2026, 42(10): 100221. doi: 10.1016/j.actphy.2025.100221 shu

Small changes, big differences: modified KSCN molten salt method for one-pot synthesis of Cd vacancy-enriched MoS₂/CdS and the enhanced photocatalytic H₂ evolution performance

Engineering Research Center of Environmental Materials and Membrane Technology of Hubei Province, School of Materials Science and Engineering, Wuhan Institute of Technology, Wuhan 430073, Hubei Province, China

Corresponding author: Xianliang Fu, Man Xu,
Received Date: 14 October 2025
Revised Date: 14 November 2025
Accepted Date: 16 November 2025

Low-temperature KSCN molten salt method has been used for one-pot fabrication of decorated sulfide-based photocatalysts. However, the reaction system is actually short of S precursor, as it is determined by the decomposition of relatively stable KSCN, which may not be conducive to the production of high-performance catalysts. To this end, a modified KSCN flux route with a dosage of external S source was developed and used for the one-pot preparation of sulfide photocatalyst with 1% MoS₂/CdS as the prototype. The results indicated that, compared with the sample (MC) prepared in conventional KSCN flux, a highly efficient sample enriched with seldom reported Cd vacancy (V_Cd, MC-S) could be readily fabricated under the S₂^--rich environment. Furthermore, both the size of CdS and MoS₂ could be substantially reduced from micrometer to nanometer scale as more nuclei could be introduced in the flux, which leads to a few-layer MoS₂ that can be uniformly and tightly anchored on CdS with the average size of only ~33 nm. Consequently, the resulting MC-S demonstrated an exceptional H₂ evolution activity of 15.01 mmol h^-1 g^-1, a significant 6.5-fold improvement over its counterpart (MC) prepared through traditional KSCN molten salt method. The high activity can be mainly ascribed to the introduction of V_Cd and the close interface between small CdS and few-layer MoS₂, which both benefit electron-hole separation. The preparation mechanism of the samples was tentatively compared and discussed from the difference in the nucleation and the development of crystals. We believe that this improved preparation method will also benefit the synthesis of other high-performance sulfide-based photocatalysts.
- Cd vacancy,
- MoS₂/CdS,
- KSCN molten salt method,
- Hydrogen evolution,
- Photocatalysis
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Small changes, big differences: modified KSCN molten salt method for one-pot synthesis of Cd vacancy-enriched MoS2/CdS and the enhanced photocatalytic H2 evolution performance

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通讯作者: 陈斌, bchen63@163.com

Small changes, big differences: modified KSCN molten salt method for one-pot synthesis of Cd vacancy-enriched MoS₂/CdS and the enhanced photocatalytic H₂ evolution performance