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Citation: Zhen Li, Sujuan Zhang, Zhongliao Wang, Jinfeng Zhang, Gaoli Chen, Shifu Chen. Rational design of S-scheme CdS/MnO2 heterojunctions for high-value photothermal synergistic catalytic oxidation of toluene[J]. Acta Physico-Chimica Sinica, ;2026, 42(4): 100179. doi: 10.1016/j.actphy.2025.100179 shu

Rational design of S-scheme CdS/MnO2 heterojunctions for high-value photothermal synergistic catalytic oxidation of toluene

  • Key Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education; School of Chemistry and Chemical Engineering, Huaibei Normal University, Huaibei 235000, Anhui Province, China

  • The targeted partial oxidation of toluene to valuable products continues to present a significant hurdle in catalytic science. To address the low efficiency of conventional photocatalysis, we developed a photothermal synergistic strategy by constructing a novel S-scheme CdS/MnO2 heterojunction catalyst. CdS nanoparticles were anchored onto MnO2, a material with intrinsic photothermal activity, forming a compact S-scheme heterojunction. This architecture generates an intrinsic electric field that markedly accelerates the segregation of light-induced charge carriers and inhibits their recombination. Moreover, CdS incorporation modulates the electronic band structure of MnO2, thereby improving product selectivity. Owing to these synergistic effects, the optimized 25% CdS/MnO2 catalyst demonstrated excellent catalytic performance, attaining a toluene oxidation rate of 14.1 mmol g−1 h−1 with an impressive 90% selectivity toward benzyl alcohol and benzaldehyde under an oxygen atmosphere at 150 ℃. Mechanistic investigations via Electron Paramagnetic Resonance and Fourier Transform Infrared Spectroscopy analyses revealed the pivotal role of photothermal synergy in promoting the oxidation process. This work not only provides an effective strategy for designing advanced photothermal heterojunctions but also presents new insights into the selective oxidation of toluene under mild conditions.
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