Citation: Ze Luo, Yukun Zhu, Yadan Luo, Guangmin Ren, Yonghong Wang, Hua Tang. Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction[J]. Acta Physico-Chimica Sinica, ;2026, 42(3): 100166. doi: 10.1016/j.actphy.2025.100166 shu

Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction

Ze Luo ¹ ,
Yukun Zhu ¹ ,
Yadan Luo ¹ ,
Guangmin Ren ² ,
Yonghong Wang ¹ ,
Hua Tang ^1,,

1.
School of Environment and Geography, College of Materials Science and Engineering, Qingdao University, Qingdao 266071, Shandong Province, China;
2.
College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao, 266042, Shandong Province, China

Corresponding author: Hua Tang, huatang79@163.com
Received Date: 16 July 2025
Revised Date: 15 August 2025
Accepted Date: 17 August 2025

Addressing the global energy and environmental crisis necessitates the development of sustainable photocatalytic technologies capable of efficiently converting biomass into high-value chemicals and clean fuels. In this study, we develop a novel one-dimensional/two-dimensional (1D/2D) In₂O₃/ZnIn₂S₄S-scheme heterojunction photocatalyst through in situ growth process. This rationally designed architecture combines rod-like In₂O₃ with sheet-like ZnIn₂S₄ nanosheets, facilitating directional charge transport and providing a high density of active sites. Consequently, the optimized In₂O₃/ZnIn₂S₄ heterojunction achieved a 5-hydroxymethylfurfural (HMF) conversion rate of 81.6% with a high selectivity of 78.2% toward 2,5-diformylfuran (DFF) and 2,5-furandicarboxylic acid (FDCA). Furthermore, it exhibited a hydrogen (H₂) evolution rate of 257.69 μmol g^-1 h^-1 under 420 nm LED irradiation. These results demonstrate the efficacy of S-scheme heterojunctions in enabling spatial charge separation and boosting photocatalytic activity, offering a promising strategy for solar-driven biomass valorization and sustainable H₂ production.
- Photocatalysis,
- S-scheme heterojunction,
- 5-hydroxymethylfurfural oxidation,
- Hydrogen evolution,
- In₂O₃/ZnIn₂S₄
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H2 evolution over In2O3/ZnIn2S4 S-scheme heterojunction

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通讯作者: 陈斌, bchen63@163.com

Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction