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Citation: Asep Bayu, Surachai Karnjanakom, Katsuki Kusakabe, Abuliti Abudula, Guoqing Guan. Preparation of Sn-β-zeolite via immobilization of Sn/choline chloride complex for glucose-fructose isomerization reaction[J]. Chinese Journal of Catalysis, ;2017, 38(3): 426-433. doi: 10.1016/S1872-2067(17)62754-2 shu

Preparation of Sn-β-zeolite via immobilization of Sn/choline chloride complex for glucose-fructose isomerization reaction

a Graduate School of Science and Technology, Hirosaki University, Hirosaki 036-8560, Japan;
b North Japan Research Institute for Sustainable Energy (NJRISE), Hirosaki University, 2-1-3, Matsubara, Aomori 030-0813, Japan;
c Department of Nanoscience, Sojo University, 4-22-1 Ikeda, Nishi-ku, Kumamoto 860-0082, Japan

Received Date: 30 September 2016
Revised Date: 23 November 2016

Well dispersion of tin species in an isolated form is a quite challenge since tin salts are easily hydrolyzed into (hydr)oxides during aqueous stannation of β-zeolite. In this study, immobilization of tin species on high silica commercial β-zeolite by using SnCl₂/Choline chloride (ChCl) complex followed with calcination provided a convenient way to get well dispersed Sn in β-zeolite in the aqueous condition, which was observed based on electron microscopy images, UV visible spectra and X-ray diffraction pattern. The existence of ChCl facilitated tin species to incorporate into zeolite. (1-2) wt% of Sn loaded β-zeolites exhibited good catalytic activity and high selectivity for glucose-fructose isomerization reaction.
- Sn-β zeolite,
- Immobilization,
- Choline chloride,
- Glucose,
- Isomerization,
- Fructose
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