Citation: Shao Hua-feng, Ma Ya-ping, Nie Hua-rong, He Ai-hua. Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1[J]. Chinese Journal of Polymer Science, ;2016, 34(9): 1141-1149. doi: 10.1007/s10118-016-1823-3 shu

Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1

Shandong Provincial Key Laboratory of Olefin Catalysis and Polymerization, Key Laboratory of Rubber-Plastics(Ministry of Education), School of Polymer Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, China

Corresponding author: Nie Hua-rong, niehr@iccas.ac.cn He Ai-hua, aihuahe@iccas.ac.cn;ahhe@qust.edu.cn
Received Date: 17 March 2016
Revised Date: 20 April 2016
Accepted Date: 20 April 2016

Fund Project: Shandong Provincial Natural Science Fund for Distinguished Young Scholars No. JQ201213the Special Foundation of Taishan Mountain Scholar Constructive Program, the National Natural Science Foundation of China No. 21174074the Nature Science Foundation of Shandong Province No. ZR2013BM004Shandong Provincical Key R & D Program No. 2015GGX102019

Solvent annealing is a facile method for changing the aggregated microstructure and physical properties of polymer materials. In this paper, we addressed the effects of solvent vapor annealing, including chloroform and water vapor, on the polymorphic transformation in both hot-pressed film and electrospun nonwoven of isotactic polybutene-1 (PB-1) by means of in situ Fourier transform infrared spectroscopy (FTIR). The pretty rapid transition rate caused by the increased motion of molecular chains under chloroform vapor is associated with a lowest crystallinity. Also, a decreased crystallinity with the crystal transition occurred in electrospun nonwovens resulting from the relaxation of the stretched molecular chains into amorphous state rather than realignment into crystal form I predominating the crystal transition process.
- Polybutene-1,
- Crystal transformation,
- Solvent vapor annealing
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