以杨絮(PC)为原料，采用乙醇溶剂热法对其进行预处理，再进行碳化，制备了高比表面积的杨絮衍生多孔碳(DPCC)，并研究了其对染料的吸附性能及动力学性能。通过单因素实验优化工艺参数，确定最佳预处理条件(液固比为17 mL·g^-1、200 ℃处理2 h)，在此条件下制备的DPCC-10比表面积达到518 m²·g^-1。结合傅里叶变换红外光谱(FTIR)、X射线衍射(XRD)、拉曼(Raman)光谱、扫描电镜(SEM)和N₂吸附-脱附测试等表征手段，证实预处理过程能够有效去除木质素和半纤维素等，形成丰富的多级孔道结构。吸附实验表明，DPCC-10对亚甲蓝(MB)的最大吸附量达到385.71 mg·g^-1，优于多数报道的生物质衍生吸附剂。DPCC-10对染料的吸附过程满足准二级动力学方程，表明该吸附以化学吸附为主。经过4次吸附-脱附循环后，DPCC-10对MB的吸附容量仍保持初始值的92.01%，表明材料具有优异的可再生性能。

To obtain materials capable of efficiently separating acetylene (C₂H₂) from carbon dioxide (CO₂) and ethylene (C₂H₄), In this work, based on the pore space partition strategy, a pacs-metal-organic framework (MOF): (NH₂Me₂)₂[Fe₃(μ₃-O)(bdc)₃][In(FA)₃Cl₃] (Fe-FAIn-bdc) was synthesized successfully by using the metal-formate complex [In(FA)₃Cl₃]^3- as the pore partition units, where bdc^2-=terephthalate, FA^-=formate. Owing to the pore partition effect of this metal-organic building block, fruitful confined spaces are formed in the network of Fe-FAIn-bdc, endowing this MOF with superior separation performance of acetylene and carbon dioxide. According to the adsorption test, this MOF exhibited a high adsorption capacity for C₂H₂ (50.79 cm³·g^-1) at 298 K and 100 kPa, which was much higher than that for CO₂ (29.99 cm³·g^-1) and C₂H₄ (30.94 cm³·g^-1) under the same conditions. Ideal adsorbed solution theory (IAST) calculations demonstrate that the adsorption selectivity of Fe-FAIn-bdc for the mixture of C₂H₂/CO₂ and C₂H₂/C₂H₄ in a volume ratio of 50∶50 was 3.08 and 3.65, respectively, which was higher than some reported MOFs such as NUM-11 and SNNU-18.