Citation: Xiu Mei TAI, Hong Xia WANG, Xiu Qi SHI. A Novel Method for the Synthesis of Mesoporous Molecular Sieve MCM-41[J]. Chinese Chemical Letters, ;2005, 16(6): 843-845. shu

A Novel Method for the Synthesis of Mesoporous Molecular Sieve MCM-41

China Research Institute of Daily Chemical Industry, Taiyuan 030001

Received Date: 15 June 2004

Fund Project: This research was supported by the National Natural Science Foundation of China (No. 20233010).

Using glycerol, glycol and water as solvent, cetyltrimethylammonium bromide (CTAB)as template, tetraethyl orthosilicate (TEOS) as silica source, ethylenediamine (EDA) as base source,mesoporous molecular sieve MCM-41 has been synthesized at room temperature, characterized by X-ray power diffraction and N₂ adsorption. Compared with the samples synthesized by glycol and water, the samples synthesized by glycerol have larger pore diameter and high surface areas.Thus glycerol is an efficient solvent for preparing larger pore mesoporous MCM-41.
- MCM-41,
- synthesis,
- glycerol,
- glycol,
- weak base,
- room temperature
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