Citation: Han Song CHEN, Xiu Fang LIU, Han Sheng XU. An Improved Synthesis of dl-Muscone[J]. Chinese Chemical Letters, ;1997, 8(1): 17-18. shu

An Improved Synthesis of dl-Muscone

Department of Chemistry, Wuhan University, Wuhan 430072

Received Date: 7 September 1996

M.Stoll's total synthetic route for dl-muscone was improved. 2.15-Hexadecanedione was synthesized by PTC method.and converted into dehydromuscones through intramolecular aldol reaction by the mixture of zinc chloride and the Grinard reagent of isoamyl bromide used as condensing agent.Catalytic hydrogenation of dehydromuscones gave dl-muscone.
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