Citation: Zhi Liang SHANG, Zhi Cai SHANG, Qing Sen YU. Synthesis of (S, S)-1, 5-bis(4-alkyl-5-hydroxy-2-oxo-3-azapentyl) 1, 5-diazacyclooctane[J]. Chinese Chemical Letters, ;2001, 12(9): 769-770. shu

Synthesis of (S, S)-1, 5-bis(4-alkyl-5-hydroxy-2-oxo-3-azapentyl) 1, 5-diazacyclooctane

Department of Chemistry, Zhejiang University, Hangzhou 310027

Received Date: 14 February 2001

Synthesis of a series of chiral aza crown ethers ((S,S)-1, 5-bis (4-alkyl-5-hydroxy-2-oxo-3-azapentyl)-1, 5-diazacyclooctane) are described.
- Chiral aza crown ether,
- 1,5-diazacyclooctane,
- synthesis
1. [1]
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14. [14]
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17. [17]
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