Citation: Man Dong GUO, Yun Long FU. Mitoxantrone Determination by 1,5-order Differential Stripping Voltammetry[J]. Chinese Chemical Letters, ;1998, 9(12): 1105-1108. shu

Mitoxantrone Determination by 1,5-order Differential Stripping Voltammetry

Department of Chemistry, Shanxi Normal University, Linfen 041004

Received Date: 16 March 1997

Fund Project: This work was supported by Natural Science Foundation of Shanxi Province.

A rapid and sensitive 1.5 order adsorptive stripping voltammetric method for determination of trace mitoxantrone (MXT) is described. The accumulation behavior of MXT on a mercury film microelectrode was studied and the possibility of carrying out 1.5 order differential adsorptive stripping analysis using mercury-coated carbon fiber microelectrode was demonstrated. Optimal conditions for 1.5 order differential voltammetry monitoring are described. The stripping peak current is linearly proportional to the concentration of MAT in the range of 1.0×10^-6mol/L-1.0×10^-9 and detection limit is 1.5×10^-10mol/L. The relative standard deviation (RSD) is 3.0% at 5.0×10^-1 (n=8). MXT can be determined directly in biological samples at physiological levels without any separation procedure.
- 1.5 order differential stripping voltammentry,
- adsorption,
- mioxantrone,
- mercury coated carbon fiber microelectrode
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