Citation: Lai Jin TLAN, Fang Xin Fu, Hua De PAN. SYNTHESIS AND CHARACTERIZATION OF THE COMPLEXES OF β-ALKOXYCARBONYLETHYLTIN TRICHLORIDES WITH DBSO AND HMPA[J]. Chinese Chemical Letters, ;1996, 7(6): 589-592. shu

SYNTHESIS AND CHARACTERIZATION OF THE COMPLEXES OF β-ALKOXYCARBONYLETHYLTIN TRICHLORIDES WITH DBSO AND HMPA

a Department of Chemistry, Qufu Normal University, Qufu, Shandong,273165;
b Department of Chemistry, Northeast Normal University, Changchun, 130024

Received Date: 17 October 1995

Fund Project: This work is supported by the National Natural Science Foundation of China.

A convenient approach based on transesterification to preparing the complexes of β-alkoxycarbonylethyltin trichlorides with dibenzylsulfoxide (DBSO) and hexamethylphosphoramide (HMPA) was reported.The structures of complexes were characterized by elemental analysis,IR,¹HNMR and X-ray single crystal diffraction.The possible mechanism for the transesterification of complexes of β-methoxycarb-onylethyltin trichloride with an alcohol was suggested.
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