Citation: Xue E WU, Chang Lu GAO, Meng Xian DING, Suo Bo ZHANG, Lian Xun GAO. A Facile Synthetic Method for Biphenyltetracarboxylic Dianhydrides[J]. Chinese Chemical Letters, ;2004, 15(7): 787-790. shu

A Facile Synthetic Method for Biphenyltetracarboxylic Dianhydrides

State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022

Received Date: 8 July 2003

Fund Project: This work was supported by the National Natural Science Foundation of China (No.20174040 and 50033010).

We report a facile and high-yielding procedure for preparing biphenyltetracarboxylic dianhydrides (BPDAs). This method relies on a nickel-catalyzed electroreductive coupling reaction of dimethyl 3-chorophthalate (3-DMCP) and/or dimethyl 4-chorophthalate (4-DMCP) with subsequent hydrolysis of tetra-ester and dehydration of tetra-acid.
- Biphenyltetracarboxylic dianhydrides,
- nickel-catalyzed,
- electroreductive coupling
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