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Citation: Liu Yumin, Zhu Kaizheng, Liu Shetian, Yie Xingkai, Wu Yue. CoCuAl Hydrotalcite-like Compounds: Synthesis and Use in the Catalytic Oxidation of p Cresol Ⅰ. Synthesis and Characterization of Hydrotalcite-like Compounds[J]. Chinese Journal of Applied Chemistry, ;1998, 15(2): 14-17. shu

CoCuAl Hydrotalcite-like Compounds: Synthesis and Use in the Catalytic Oxidation of p Cresol Ⅰ. Synthesis and Characterization of Hydrotalcite-like Compounds

Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022

Received Date: 24 September 1997
Revised Date: 10 December 1997

The hydrotalcite-like compounds CoMAlCO₃(HTLc,M=Cu²⁺, Ni²⁺,Mn²⁺,Cr³⁺,Fe³⁺) were synthesized by coprecipitation method and characterized by XRD and IR measurements. The results showed that the interlayer H₂O and OH^- and CO₃^2- in the compounds were lost with the increase of the calcination temperature, with the structure of the compounds being changed into spinel structure. The CO₂ TPD results showed that the calcination temperature and Co/Cu ratio of the compounds had an obvious effects on the surface area and the alkalinity of the products.
- CoCuAlCO₃,
- hydrotalcite compound,
- synthesis,
- characterization
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