Citation: Lian She FU, Qing Hong XU, Hong Jie ZHANG, Lian Sheng LI, Jia Zuan NI, Ru Ren XU. Preparation and Characterization of Layered Compound Zirconium Bis(monohydrogenphosphate) Intercalated with Rare Earth Complex[J]. Chinese Chemical Letters, ;2000, 12(2): 171-174. shu

Preparation and Characterization of Layered Compound Zirconium Bis(monohydrogenphosphate) Intercalated with Rare Earth Complex

1.
Key Laboratory of Rare Earth Chemistry & Physics Changchun Institute of Applied Chemistry Chinese Academy of Sciences Changchun 130022;
2.
Key Laboratory of Inorganic Synthesis & Preparative Chemistry Chemistry Department of Chemistry Jilin Uuiversity Changchun 130023

Received Date: 31 August 1999

Fund Project: National Noble Youth Fund of Sciences(No.29225102) and the National Natural Science Foundation of China for financial support of this work.the National Natural Science Key Foundation of China(No.29731010)We are grateful to the National Key Project for Fundamental Research

Layered compound zirconium bis(monohydrogenphosphate)(α-ZrP) intercalated with rare earth complex Eu(DBM)₃phen was prepared.The pre-intercalation of p-methoxyaniline into α-ZrP makes the interlayer separation large enough to exchange PMA with europium complex, thus, the luminescent assembly was prepared.This was confirmed by X-ray diffraction, UV-visible spectra and elemental analysis.The fluorescence spectra and lifetime of the assembly were also presented.
- Layered compound, rare earth complex, luminescence.
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