Citation: Dun Qing WANG, Dai Rong CHEN, Xiu Ling JIAO. Synthesis of Nickel Sulfide Particles by Solvothermal Process[J]. Chinese Chemical Letters, ;2004, 15(1): 79-82. shu

Synthesis of Nickel Sulfide Particles by Solvothermal Process

1.
Department of Chemistry, Shandong University, Jinan 250100;
2.
Department of Chemistry, Dezhou College, Dezhou 253000

Received Date: 20 December 2002

Pyrite nickel disulfide and millerite nickel monosulfide have been successfully prepared by solvothermal method based on the reaction of Ni(NO₃)₂·6H₂O and H₂NC(S)NH₂ in benzene and ethylenediamine (EDA). The final products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM). The effects of the solvent, reaction temperature and time on the morphology and phase of the products have been discussed.
- Chalcogenides,
- solvothermal synthesis,
- X-ray diffraction analysis
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