Citation: Jin-Xian WANG, Chin-Hsien WANG, Wen feng CUI, Yu lai HU, Kai ZHAO. STUDIES ON THE REACTION OF SULFUR, SELENIUM AND TELLURIUM WITH SODIUM HYDROXIDE UNDER PHASE TRANSFER CATALYSIS(Ⅱ).A CONVENIENT METHOD FOR THE SYNTHESIS OF BI(ACYL)DISULFIDES[J]. Chinese Chemical Letters, ;1990, 1(3): 193-196. shu

STUDIES ON THE REACTION OF SULFUR, SELENIUM AND TELLURIUM WITH SODIUM HYDROXIDE UNDER PHASE TRANSFER CATALYSIS(Ⅱ).A CONVENIENT METHOD FOR THE SYNTHESIS OF BI(ACYL)DISULFIDES

Institute of Chemistry Department of Chemistry Northwest Normal University Lanzhou 730070

Received Date: 16 January 1990

Fund Project: We wish to thank the Gansu Science Foundation of China for partial financial support.

A simple and general method for the synthesis of bi(acyl)disulfides isreported.Sulfur is allowed to react with sodium hydroxide to give sodium disulfideat 65℃ under PTC, which can react with acyl halides to afford bi(acyl)disulfides ingood to excellent isolated yields.The effects of solvents and phase transfercatalysts are discussed.
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