Citation: Lu Ling WU, Xian HUANG. SYNTHESIS AND APPLICATION OF VINYL DITHIOCARBAMATES[J]. Chinese Chemical Letters, ;1995, 6(9): 751-752. shu

SYNTHESIS AND APPLICATION OF VINYL DITHIOCARBAMATES

Lu Ling WU ,
Xian HUANG

Department of Chemistry, Hangzhou University, Hangzhou 310028

Received Date: 26 January 1995

Fund Project: Supported by Natural Science Foundation of China.

In the presence of potassium t-butoxide, N, N-dimethylamino thiocarbonyl thiomethyl triphenylphosphonium bromide formed the corresponding ylide in situ, which can undergo Wittig reaction with aldehydes to give vinyl dithiocarbamates in high yields.If the esters were hydrolyzed with ethanol aqueous sodium hydroxide, a new method to lengthen aldehydes by one carbon atom was a-complished.
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