Citation: AN Zhe, GAO Jing, ZHU Ling. Synthesis, Crystal Structure and Photoluminescent Property of a New Ca(Ⅱ) Compound Constructed from 5-Oxyacetateisophthalic Acid[J]. Chinese Journal of Structural Chemistry, ;2014, 33(7): 1063-1068. shu

Synthesis, Crystal Structure and Photoluminescent Property of a New Ca(Ⅱ) Compound Constructed from 5-Oxyacetateisophthalic Acid

AN Zhe ^a ,
GAO Jing ^b ,
ZHU Ling ^a,,

a.
a. School of Chemistry Life and Science, Guangdong University of Petrochemical Technology, Maoming, Guangdong 525000, China;
b.
b. College Department of Pharmacy, Mudanjiang Medical University, Mudanjiang, Heilongjiang 157011, China

Corresponding author: ZHU Ling,
Received Date: 2 January 2014
Available Online: 12 May 2014
Fund Project: Supported by the Program for Talent Introduction in Guangdong Higher Education Institutions (No. 201242) (No. 201242)the Scientific Research Start-up Funds for Talent Introduction in Guangdong University of Petrochemical Technology (No. 510018) (No. 510018)

A new coordination polymer, namely [Ca(HOABDC)]_n (1, H₃OABDC=5-oxyacetateisophthalic acid), has been synthesized through hydrothermal reactions of Ca(NO₃)₂ and H₃OABDC. The title compound crystallizes in monoclinic, space group P2₁/c with a=4.3043(2), b=21.4959(11), c=10.7450(6) Å, β=91.411(5)°, V=993.88(9) Å³, C₁₀H₆O₇Ca, M_r=278.23, Z=4, D_c=1.859 g/cm³, F(000)=560, μ=0.659 mm^-1, the final R=0.0328 and wR=0.0670 for 1469 observed reflections (I>2σ(I)). Single-crystal X-ray structural analysis reveals that compound 1 features 1D Ca(Ⅱ)-carboxylate chain-shaped subunits, which are further connected together via HOABDC^2- ligands into a 3D (6,6)-connected nia-type hybrid framework. Moreover, the luminescent property and thermal stability of 1 were also investigated.
- calcium(Ⅱ),
- 5-oxyacetateisophthalic acid,
- luminescence,
- metal-carboxylate chain
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