Citation: Zhong Xu LIU, Yong Kui SHAN, En Bo WANG, Zhong Sheng JIN, Ge Cheng WEI, Yong Sheng LIU. CRYSTAL STRUCTURE OF POTASSIUM 9-MOLYBDO-3-VANADOPHOSPHATE[J]. Chinese Chemical Letters, ;1991, 2(2): 179-180. shu

CRYSTAL STRUCTURE OF POTASSIUM 9-MOLYBDO-3-VANADOPHOSPHATE

a Changchun Harbin Normal University, Harbin 150030;
b Northeast Normal University, Changchun 130024;
c Institute of Applied Chemistry, Academia Sinica, Changchun 130022

Received Date: 11 June 1990

K₄H₂PMo₉V₃O₄₀·18H₂O, Mr=2169.68, tetragonal, space group P4/mnc, a=b=12.515 (3), c=17.636 (7) A;z=2;V=2762 (2) A³;F (000)=2206;Dc=2.81g/cm³;μ=28.8/cm (MoKα=0.71069 A). The central PO₄ is disordered in the (PMo₉V₃O₄₀) ⁶. P-O=1.511A. M (M=Mo or V) is 7 coordinate, M-O=1.62-2.48A. K is 7 coordinate, K-O=2.85-3.10A.
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