Citation:
Ding Liming, Lin Yunqing, Qi Li, Zhou Zinan, Wang Fosong. Studies of Solid Polymer ElectrolytesⅠ.Synthesis and Characterization of A Novel Comblike Copolymer with Oligo-Oxyethylene Side Chains[J]. Chinese Journal of Applied Chemistry,
;1994, 11(6): 41-44.
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A comblike polymer based on methyl vinyl etherlmaleic anhydride copolymer backbone and with oligo-oxyetllylene side chins was synthesized for the first time.A two-step esterification has been carried out for polymer synthesis:reacting maleic anhydride with PEGME in methylethyl ketone at 80℃ for 24hurs and then reacting the product obtained with methanol in the presence of p-toluene sulfonic acid at 60℃ for 24 hours.The structure of the product was confirmed by IR,13C NMR and elemental analysis.
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