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Citation: Zhao Daqing, Zhang Jianguo, Wu Yijie, Pei Fengkui, Qiu Shilun, Pang Wenqin. SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA[J]. Chinese Journal of Applied Chemistry, ;1993, 10(2): 17-19. shu

SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA

1.
1. Changchun Institute of Applied Chemistry, Chinese, Academy of Sciences, 130022 Changchun;
2.
2. Department of Chemistry, Jilin University, 130022 Changchun

Received Date: 29 January 1992
Available Online: 19 May 1992

Hydrothermal crystallization of silica zeolite from nonalkaline media containing F^-anions has been investigated. The MFI type (ZSM-5) silica zeolites were obtained with tripropylamine,choline, 1,4-diazabicyclo[2,2,2]octane or piperazine as template. Silica Thetα-1 and ZSM-39 were prepared using 1,6-diaminohexane and tetramethylamminum cation as template, respectively. Highly resolved ²⁹Si MAS NMR spectra of silica zeolites from nonalkaline media reveal new feature of the materials, which are indicative of the very low defect content and very high crystallinity.
- silica zeolite,
- synthesis,
- characterization
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