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Citation: ZHONG Ming, YI Zhi-Qun, ZHAN Yu-Lin, WEN Hong-Li, SONG Cai-Sheng. Synthesis and Properties of Poly(ether ether ketone) Containing Imide Moiety[J]. Chinese Journal of Applied Chemistry, ;2009, 26(11): 1273-1276. shu

Synthesis and Properties of Poly(ether ether ketone) Containing Imide Moiety

1.
School of Chemistry & Chemical Engineering, Jiangxi Normal University, Nanchang 330022

Corresponding author: SONG Cai-Sheng,
Received Date: 28 October 2008
Available Online: 19 April 2009
Fund Project: “十一五”军品配套项目(JPPT-115-643) (JPPT-115-643)科技型中小企业技术创新基金(06C26213601342) (06C26213601342)

Two novel poly(ether ether ketone)s(PEEK) containing imide moiety with inherent viscosities of 0.98 dL/g and 0.61 dL/g were respectively prepared by low temperature solution polycondensation from 1,4-diphenylbenzene(DPB) with N,N'-(4,4'-diphenylmethane) bistrimelletimide diacid chloride(DCDI-M) or N,N'-(4,4'-diphenylsulfone) bistrimelletimide diacid chloride(DCDI-S).The polymers were characterized by FT-IR,¹H NMR,DSC,TGA and WAXD.The results show that the polymers are amorphous.The glass transition temperatures(T_g) are 236 ℃ and 263 ℃,respectively.The onset temperatures taken at a 5% mass loss of each of the polymers in nitrogen atmosphere are all over 512 ℃.The polymers are soluble in common organic solvents such as N,N-dimethylacetamide(DMAc),N-methylpyrrolidone(NMP),cresol and chloroform at room temperature.
- imide moiety,
- diphenoxylbenzene,
- poly(ether ether ketone)
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