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Citation: LI Xia, XIONG Yuan-Fu, WEN Zhu-You, JIANG Li-Hua, ZHU Hong-Fu. Purification of Lycorine from Lycoris Herb. by Macroporous Adsorbent Resin[J]. Chinese Journal of Applied Chemistry, ;2009, 26(3): 325-328. shu

Purification of Lycorine from Lycoris Herb. by Macroporous Adsorbent Resin

1.
a College of Science, Hunan Agricultural University, Changsha 410128;
2.
b College of Animal Science and Technology, Hunan Agricultural University, Changsha 410128

Corresponding author: XIONG Yuan-Fu,
Received Date: 12 February 2008
Available Online: 27 May 2008
Fund Project: 湖南农业大学人才基金资助项目(04WD12) (04WD12)

To study the conditions and parameters for the purification of lycorine with macroporous adsorbent resin,the adsorption and desorption of nine macroporous adsorbent resins for lycorine were compared.The optimal adsorbent HPD300 and the appropriate adsorption/desorption conditions were determined,i.e.,the concentration of lycorine in extract solution was at 1.22 g/L,volume at 9BV was passed through the column at a flow rate of 2 BV/h and room temperature,the column was washed with 4 BV water at a flow rate of 2 BV/h,8 BV 70% alcohol was satisfactory eluant for desorption at a flow rate of 2 BV/h.The purity of lycorine was increased from 9.93% to 23.07%.
- lycoris herb.,
- lycorine,
- macroporous adsorbent resin,
- purification
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