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Citation: SONG Li, SONG Mei-Rong, LI Qing-Hua, ZHANG Zhi-Jun. Preparation and Characterization of Iron Nanoparticles and Application in Kerosene[J]. Chinese Journal of Applied Chemistry, ;2009, 26(2): 202-205. shu

Preparation and Characterization of Iron Nanoparticles and Application in Kerosene

1.
a Key Laboratory for Special Functional Materials, Henan University, Kaifeng 475001;
2.
b College of Science, Henan Agricultural University, Zhengzhou

Corresponding author: ZHANG Zhi-Jun,
Received Date: 21 January 2008
Available Online: 28 April 2008
Fund Project: 国家自然科学基金(50701016)资助项目 (50701016)

Fe nanoparticles were prepared by reducing Fe²⁺ salt in an ethanol solution with NaBH₄ in the presence of 2 Ethy hexanoic acid as a surfactant.The structure,morphology and thermal properties of the iron nanoparticles were investigated by means of X-ray diffraction(XRD),transmission electron microscopy(TEM),oxygen bomb calorimeter and themogravimetry(TG).The results showed that the crystal are body-centered-cubic,the particles are spherical with an average size of approximate 100 nm,and there is conglutination among the particles.The thermal property studies indicated that the mass of Fe increased from 22% to 28%,before and after using surfactant in a temperature range of 25～600 ℃,which showed that the anti-oxidation properties was improved distinctly after using surfactant.When the amount of Fe in Kerosene was less than 1%(mass ratio),the combustion heat value of the Kerosene would be enhanced and the maximum was approximately 234.08 J/g.
- liquid chemical reduction method,
- iron nanoparticles,
- combustion heat
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