Citation:
JING Xiao-Yan, KUANG Wei-Wei, LIU Jing-Yuan, YU Fang. Synthesis and Photoluminescence of ZnO Nanorods Prepared by Alcohol Thermal Method[J]. Chinese Journal of Applied Chemistry,
;2009, 26(1): 90-93.
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Crystalline ZnO nanorods were prepared by means of a simple one-step alcohol thermal approach with oleic acid(OA) as a stabilizing agent under atmospheric pressure.The OA-stabilized ZnO nanorods were characterized by XRD,SEM,TEM,HRTEM and FT-IR.PL spectrum of the product after annealing was studied,and the growth mechanism of ZnO nanorods was also discussed.The results showed that the nanorods grow along the direction with a diameter of 10~15 nm and a length of 150~200 nm,and the binding of OA with ZnO nanorods was confirmed by FTIR.The obtained ZnO nanorods exhibited good near-UV emission properties.With the increase of the annealing temperature,the intensity of the deep-level emission decreased and then increased.
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Keywords:
- ZnO,
- nanorods,
- photoluminescence,
- annealing
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