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Citation: WANG Ming-Xing, SONG Xi-Ming, ZHANG Shu-Fen, YANG Jin-Zong, LÜ Ting-Qiao. Synthesis of Benzyl p-hydroxybenzoate[J]. Chinese Journal of Applied Chemistry, ;2001, 18(4): 327-328. shu

Synthesis of Benzyl p-hydroxybenzoate

1.
a State Key Laboratory of Fine Chemicals, Dalian University of Science and Technology, Dalian;
2.
b Department of Chemistry, Liaoning University, Shenyang 110036

Received Date: 30 May 2000
Available Online: 11 September 2000
Fund Project: 辽宁省优秀青年科技人才培养基金(973007) (973007)

Benzyl p-hydroxybenzoate was prepared from benzyl chloride and p-hydroxybenzoic acid by phase transfer catalysis, in which xylene was used as an organic solvent, Na₂CO₃ aqueous solution as a condensing agent and Bu₄NCl as a phase transfer catalyst. The effects of reaction time, Na₂CO₃ concentration and feed amount of raw materials were investigated. The concentration of Na₂CO₃ aqueous solution was the most important factor. Prodact with purity greater 98% and yield more 85% was obtained.
- benzyl p-hydroxybenzoate,
- preperation,
- PTC
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