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Citation: XU Hai, YU Dao-Yong, SUI Xiu-Hua, QUE Guo-He. Isolation and Characterization of Metalloporphyrin from Liaohe Oil Residue[J]. Chinese Journal of Applied Chemistry, ;2001, 18(5): 419-421. shu

Isolation and Characterization of Metalloporphyrin from Liaohe Oil Residue

1.
College of Chemistry and Chemical Engineering, University of Petroleum, Dongying 257061

Received Date: 29 December 2000
Available Online: 12 March 2001

In Liaohe oil residue nickel content is high and vanadium content is low. There are some kinds of metalloporphyrin in Liaohe oil residue. In this paper the nickel porphyrin is isolated by extraction with acetonitrile. The isolated nickel porphyrin has a characteristic peak at 552 nm, by which the concentration of nickel as porphyrins is determined. The nickel porphyrin is dematallated with methanesulfonic acid. The demetallated porphyrin has four peaks in visible band with Ⅳ> Ⅲ> Ⅱ> Ⅰ. This shows ETIO is the main porphyrin compound in Liaohe oil residue.
- Liaohe oil residue,
- porphyrin,
- isolation,
- characterization
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