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Citation: WANG Shu-Jun. Study on the Carbonized Poly(p-phenylene) Resin for Electrode Materials of Lithium Ion Battery (Ⅰ). The Composition and Structure of the Carbonized Resin[J]. Chinese Journal of Applied Chemistry, ;2001, 18(11): 889-892. shu

Study on the Carbonized Poly(p-phenylene) Resin for Electrode Materials of Lithium Ion Battery (Ⅰ). The Composition and Structure of the Carbonized Resin

WANG Shu-Jun

1.
Institute of Chemical Engineering, University of Petroleum Beijing Campus, Beijing 102200

Received Date: 30 November 2000
Available Online: 30 August 2001

The temperature and atmosphere of heat treatment showed important effects on the carbon and hydrogen contents in final carbonized poly(p-phenylene) resin. The carbon contents of samples treated in an inert atmosphere were lower than those of samples treated in reductive atmosphere at the same temperatures; but hydrogen contents of samples were just the opposite to it. And the samples treated at 1 000℃ still contained hydrogen. The specific surface areas of samples treated at 1 000℃ in an inert atmosphere dropped to 15 6% as compared with those for the sample treated at 1 000℃ in reductive atmosphere. The specific surface areas of carbonized product decreased with increase in carbonization temperature. The IR and X-ray diffraction spectral analysis showed that the samples treated at 700℃ began to form fused benzene ring structure, but the carbons still belong to amorphous carbon. At 1 000℃ there appeared some graphite characteristic diffraction peaks in XRD spectra and higher graphitization level.
- poly(p-phenylene),
- carbonization,
- elemental content,
- structure
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