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Citation: CUI Yun-Mei, JIN Bao-Kang. Fabrication and Evaluation of a Double Transparent Windows, Double-walled IR Reflected Thin Layer Electrochemical Cell[J]. Chinese Journal of Applied Chemistry, ;2003, 20(12): 1166-1170. shu

Fabrication and Evaluation of a Double Transparent Windows, Double-walled IR Reflected Thin Layer Electrochemical Cell

CUI Yun-Mei ,
JIN Bao-Kang ^,

1.
School of Chemistry and Chemical Engineering, Anhui University, Hefei 230039

Corresponding author: JIN Bao-Kang,
Received Date: 24 April 2003
Available Online: 22 September 2003
Fund Project: 安徽省自然科学基金(99046129) (99046129)安徽省教委自然科学基金(99JL0024)资助项目 (99JL0024)

A double transparent window, double-walled IR reflected thin layer electrochemical cell is described. The cell is fit for both aqueous system and non-aqueous system. The results of electrochemical evaluation of K₄Fe(CN)₆ aqueous solution and catechol、hydroquinone in acetonitrile solution showed that the impedance effect and edging effect of the cell could be controlled to a great degree. In the spectra of in-situ FTIR spectroelectrochemical evaluation for cell in aqueous K₄Fe(CN)₆ solution, the negative-going C-N peak of Fe(CN)₆^3- and the positive-going C-N peak of Fe(CN)₆^4- were observed clearly during the oxidation process, in accordance with that reported in literatures. Meanwhile, at the low-temperature in-situ FTIR spectroelectrochemical experiment of hydroquinone in acetonitrile solution using liquid N₂ as refrigerant the clear redox IR spectra with good signal-noise ratio were also obtained.
- thin layer electrochemical cell,
- double window,
- in-situ FTIR spectroelectrochemitry,
- K₄Fe(CN)₆,
- hydroquinone
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