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Citation: SUN Cai-Ying, LI Bin, ZHANG Zhuan-Fang, SHAO Bo, XU Shu-Cai. Synthesis and Characterization of Bis-phenol Ester of Spirocylic Pentaerythritol Bis-chlorophosphatidic Acid[J]. Chinese Journal of Applied Chemistry, ;2006, 23(2): 165-168. shu

Synthesis and Characterization of Bis-phenol Ester of Spirocylic Pentaerythritol Bis-chlorophosphatidic Acid

1.
Department of Chemistry, University of Northeast Forestry, Harbin 150040

Corresponding author: LI Bin,
Received Date: 8 April 2005
Available Online: 2 August 2005
Fund Project: 黑龙江省自然科学基金(9805) (9805)

With water as solvent,the bis-phenol ester of spirocylic pentaerythritol bischlorophosphatidic acid was prepared from spirocyclic pentaerythritol bis-chlorophosphatide and phenol under alkaline condition.The reaction time was determined by monitering the reaction process with the absorbency variation of phenol sodium in the reaction system at 269.6 nm.The product structure was characterized with FTIR,¹H NMR and the phosphorus amount.The thermal stability of the product was analysed with TG measurement.
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