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Citation: LIU Rong-Fang, XIAO Xiu-Feng. Hydrothermal Electrodeposition and Properties of Hydroxyapatite/Zirconia Composite Coatings[J]. Chinese Journal of Applied Chemistry, ;2006, 23(6): 612-616. shu

Hydrothermal Electrodeposition and Properties of Hydroxyapatite/Zirconia Composite Coatings

LIU Rong-Fang ^, ,
XIAO Xiu-Feng

1.
College of Chemistry and Material Science, Fujian Normal University, Fuzhou 350007

Corresponding author: LIU Rong-Fang,
Received Date: 26 June 2005
Available Online: 30 January 2006
Fund Project: 福建省发改委(2004[477]) (2004[477])福建省自然科学基金(E02100018)资助项目 (E02100018)

HA/ZrO₂ composite coatings were successfully prepared on titanium electrode by means of the hydrothermal electrodeposition method via adding ZrO₂ powder in the electrolyte in an autoclave.The bonding strength,bioactivity and thermal stability of the coatings were investigated.The results obtained show that the bonding strength of HA/ZrO₂ composite coating is obviously higher than that of pure HA coating.HA/ZrO₂ composite coating surfaces are covered by carbonate-apatite coating after immersion in simulate body fluid for 7 d,which indicates that the bonding strength of the coating is improved without the decrease of the bioactivity by the addition of the ZrO₂ in HA coating.Tetragonal phase ZrO₂(t-ZrO₂) underwent a martensitic transformation to monoclinic phase ZrO₂(m-ZrO₂) after sintering treatment.At sintering temperature above 700℃,HA partially decomposed which causes the ZrO₂ transformation to β-calcium phosphate(β-TCP).when sintering at 1 200℃,HA decomposed to α-calcium phosphate(α-TCP) and gave CaO,cubic phases ZrO₂ (c-ZrO₂) and yields CaZrO₃.
- hydrothermal electrodeposition,
- hydroxyapatite,
- ZrO₂,
- bonding strength,
- bioactivity
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