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Citation: LIU Shu-Fen, HU Yu-Cai, MA Song-Mei, LI Gui-Hua, FANG Xin-Qiang, ZHENG Ke. Synthesis and Adsorption Properties of a Novel Polymer Containing Cyclic Pseudo-Cryptand Ether as Functional Group for Fe³⁺[J]. Chinese Journal of Applied Chemistry, ;2006, 23(7): 753-756. shu

Synthesis and Adsorption Properties of a Novel Polymer Containing Cyclic Pseudo-Cryptand Ether as Functional Group for Fe³⁺

1.
a School of Chemistry and Material Science, Yantai Normal University, Yantai 264025;
2.
b School of Chemistry and Material, Chinese Technology University, Hefei;
3.
c Yantai Institute of Natural Gas, Yantai

Corresponding author: LIU Shu-Fen,
Received Date: 26 August 2005
Available Online: 22 February 2006
Fund Project: 山东省优秀中青年科学家科研奖励基金(2004BSO8001) (2004BSO8001)

With 2-phenoxyethanol as initial material,a novel pseudo-cryptand ether polymer with crosslinking phenolic chain and nitrogen atom at the end of bridge was synthesized by a combined method of first polymerization,then cyclization and functionalization.Static adsorption properties of the polymeric cryptand ether for metallic ions were tested.The results show that the polymer has a good preferential adsorption property for Fe³⁺ and the adsorption capacity is 1.22 mmol/g(start concentration of Fe³⁺:0.053 mol/L,25℃).Within the limits,the quantity of adsorption for Fe³⁺ increases along with the rising of Fe³⁺ concentration and the increase of adsorptive time,the adsorption reaches equilibrium after three hour.The polymer has a good reprocess property and it can be fully reused.The adsorption capacities were over 1.16 mmol/g after it was used more than four times.
- polymeric pseudo-cryptand ether,
- synthesis,
- adsorption
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Synthesis and Adsorption Properties of a Novel Polymer Containing Cyclic Pseudo-Cryptand Ether as Functional Group for Fe3+

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Synthesis and Adsorption Properties of a Novel Polymer Containing Cyclic Pseudo-Cryptand Ether as Functional Group for Fe³⁺