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Citation: LI Fang, CHEN Jia-Sheng, LIU Fang-Ming, XIE Zheng-Feng. Synthesis of Carboxaldehyde Hydrazone Derivatives Containing 1H-1,2,4-triazole and Thiazole[J]. Chinese Journal of Applied Chemistry, ;2007, 24(1): 108-110. shu

Synthesis of Carboxaldehyde Hydrazone Derivatives Containing 1H-1,2,4-triazole and Thiazole

1.
a College of Chemistry and Chemical Engineering, Xinjiang University, Ulumqi 830046;
2.
b Department of Chemistry, Hangzhou teaching College, Hangzhou 310012

Corresponding author: LIU Fang-Ming,
Received Date: 15 January 2006
Available Online: 12 April 2006
Fund Project: 国家自然科学基金(29702007,20162004)资助项目 (29702007,20162004)

A series of new carboxaldehyde thiosemicarbazones was synthesized by the condensation reaction of 2-phenyl-1,2,3-triazol-4-carboxaldehyde with thiosemicarbazide, the product reacted with five substituted α-bromoacetophenone or α-bromo-α-(1H-1,2,4-triazol-1-yl) acetophenone subsequently in EtOH under refluxing to afford a series of carboxaldehyde hydrazone derivatives.Their structures were confirmed by elemental analysis, IR, ¹H NMR, and MS spectra.The biological test results show that most of these compounds have no antiviral and fungicidal activity.
- triazole,
- thiazole,
- carboxaldehyde hydrazone
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