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Citation: ZHENG Bo, MA Mei-Hua, GU Jian-Sheng. Electrochemical Synthesis of Antimony Oxychloride Sb₄O₅Cl₂[J]. Chinese Journal of Applied Chemistry, ;2007, 24(2): 226-228. shu

Electrochemical Synthesis of Antimony Oxychloride Sb₄O₅Cl₂

1.
a Institute of Applied Chemistry, Nanjing Xiaozhuang University, Nanjing 210017;
2.
b Department of Chemistry and Chemical Engineering, Suzhou University, Suzhou

Corresponding author: ZHENG Bo,
Received Date: 20 March 2006
Available Online: 10 June 2006
Fund Project: 南京晓庄学院青年专项基金(2005NXY45) (2005NXY45)

The antimony oxychloride was synthesized by means of electrochemical method.The anode comprised of sacrificial metal Sb;the cathode was an indifferent conducting material;the electrolyte could be a chloride salt soluble in the hydrochloric acid.Uhrafine metal Sb(10nm) was directly prepared by elec-trosynthesis,and antimony oxychloride was synthesized through hydrolyzing antimony chloride solution which was formed by the reaction of ultrafine Sb and hydrochloric acid.The synthetic condition was discussed and the structure and morphology of the product were characterized by virtue of titration,XRD,SEM and TEM.The synthetic process is simple without contamination.
- antimony oxychloride,
- electrochemistry,
- synthesis,
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Electrochemical Synthesis of Antimony Oxychloride Sb₄O₅Cl₂