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Citation: CHEN Zheng-Guo, WANG Hai-Ping, PAN Shou-Wei. Synthesis and Dynamic Surface Tension of New Sulfonated Polyether Surfactant[J]. Chinese Journal of Applied Chemistry, ;2007, 24(2): 168-172. shu

Synthesis and Dynamic Surface Tension of New Sulfonated Polyether Surfactant

1.
Faculty of Chemistry and Material Science Hubei University, the Hubei Province Key Laboratory of Polymer Materials, Wuhan 430062

Corresponding author: CHEN Zheng-Guo,
Received Date: 8 March 2006
Available Online: 30 June 2006
Fund Project: 湖北省教育厅自然科学重点研究资助项目(99A001) (99A001)

Four amphiphilic copolymers of 3-chloro-2-hydroxy-1-propanesulfonate sodium(NaCHPS) and 1-chloro-3-butoxy-2-propanol(CBP) were prepared via base-catalyzed polycondensation.The copolymers were characterized by means of FT-IR,¹H and ¹³C NMR analysis.Vapor Pressure Osmometry(VPO) indicated the total number average molecular weights were in the range of 900~1600.The dynamic surface tension(DST) of sulfonated polyether aqueous solution with different mass concentrations and structures was measured via the plate method.The results show that when the mass concentration increases from 56.4 mg/L to 3 611 mg/L, the value of R_1/2 increases from 11.04 mN/(m·min) to 7 662.5 mN/(m·min).Dynamic surface activity of sulfonated polyether increases with increasing sulfonated polyether concentration and 1-chloro-3-butoxy-2-propanol(CBP) unit.
- polymeric surfactant,
- sodium chlorohydroxypropanesulfonate,
- chlorobutoxypropanol,
- synthesis,
- dynamic surface tension
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