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Citation: CHENG Kang-Min, SHEN Yu-Mei, WANG Mou-Hua, FENG Cui-Lan. Synthesis of β-Elemene Amino Acid Derivatives[J]. Chinese Journal of Applied Chemistry, ;2008, 25(5): 560-563. shu

Synthesis of β-Elemene Amino Acid Derivatives

1.
Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800

Corresponding author: SHEN Yu-Mei,
Received Date: 23 May 2007
Available Online: 24 September 2007
Fund Project:

A series of β-elemene monosubstituted amino acid derivatives were synthesized from the reaction of β-elemene with each of seven different amino acids under basic condition at 66℃,and their structures were characterized by IR,¹H NMR,and HRMS.Sodium hypochloride added in this step should be 2 equivalent of the reacted β-elemene.The β-elemene monosubstituted amino acid derivatives were prepared from the unprotected amino acids with ethanol and water as solvent (V(EtOH):V(H₂O)=4:1).The effects of temperature on reaction yield showed that more byproducts would appear at higher temperatures and the reaction would run much slower at low temperatures.
- β-elemene,
- derivatives,
- amino acid
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