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Citation: ZHU Chuan-Gao, XU Bo, WANG Feng-Wu. In situ Preparation of Nano-SnO₂ in HOCH₂CH₂OH[J]. Chinese Journal of Applied Chemistry, ;2008, 25(12): 1493-1495. shu

In situ Preparation of Nano-SnO₂ in HOCH₂CH₂OH

1.
Department of Chemistry, Huainan Normal College, Huainan 232001

Corresponding author: ZHU Chuan-Gao,
Received Date: 18 November 2007
Available Online: 8 May 2008
Fund Project: 安徽省高校自然科学基金资助项目(KJ2007B339ZC,KJ2007B162) (KJ2007B339ZC,KJ2007B162)安徽省自然科学基金重点项目(070414270X) (070414270X)

Sn complex Sn(OCH₂CH₂O)₂ was directly synthesized in HOCH₂CH₂OH solution in 50 mL flask.The nano-SnO₂ powder was prepared by a direct sol-gel of the above solution followed by dryness at 350℃ for 2 h.The product Sn(OCH₂CH₂O)₂ was characterized by FT-IR,Raman and NMR.XRD,and TEM were used to investigate the structure of nano-SnO₂.The experiments show Sn(OCH₂CH₂O)₂ contained-OCH2CH2O-group and could prevent the precursor from aggregating during the process of hydrolysis and calcination.The nano-SnO₂ with a diameter of 10~30 nm was thus obtained in a high purity.
- HOCH₂CH₂OH,
- stannum complex,
- sol-gel,
- nano-SnO₂
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In situ Preparation of Nano-SnO₂ in HOCH₂CH₂OH