Citation: NIE Xu-Liang, XIONG Hui, TU Yong-Gang, HUANG Chang-Gan. Synthesis and Crystal Structures of Complexes of Copper, Silver Assembled by Diniconazole[J]. Chinese Journal of Inorganic Chemistry, ;2012, 28(12): 2593-2596.
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Two new complexes [CuL4Cl2] (1) and [AgL2]NO3 (2) (L=diniconazole) were synthesized by solvothermal condition and structurally characterized by element analysis, IR and single crystal X-ray diffraction. Complex 1 is the Triclinic system, space group P1 with a=0.882 3(7) nm, b=1.370 5(10) nm, c=1.516 4(11) nm, α=91.507(11)°, β=97.356(9)°, γ=107.683(9)°. Complex 2 belongs to the Monoclinic system, space group P21/c with a=1.229 2(3) nm, b=1.272 1(3) nm, c=2.431 7(5) nm, α=90°, β=98.694(3)°, γ=90°. 1 and 2 are linked into a one dimensional chain by intermolecular hydrogen bonds. CCDC: 805738, 1; 818240, 2.
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