Citation: Guan-Jie Wang, Mei-Ling Qi. Analysis of volatile compounds in Herba Asari by single-drop micro-extraction gas chromatography mass spectrometry[J]. Chinese Chemical Letters, ;2013, 24(6): 542-544. shu

Analysis of volatile compounds in Herba Asari by single-drop micro-extraction gas chromatography mass spectrometry

Guan-Jie Wang ^a ,
Mei-Ling Qi ^b,,

1.
a National Institutes for Food and Drug Control, Beijing 100050, China;
2.
b School of Chemistry, Beijing Institute of Technology, Beijing 100081, China

Corresponding author: Mei-Ling Qi,
Received Date: 7 January 2013
Available Online: 26 February 2013

A rapid headspace single-drop micro-extraction (mix) gas chromatography mass spectrometry (SDME-GC-MS) for the analysis of the volatile compounds in Herba Asari was developed in this study. A mixed solvent of n-tridecane and butyl acetate (1:1) was finally used for the extraction at 70 ℃ for 15 min with sample amount of 0.750 g and 100 mesh particle size. Under the determined conditions, the pound samples of Herba Asari were directly applied for the analysis. SDME-GC-MS, SPME-GC-MS and SD-GC-MS methods were compared and the results showed that SDME-GC-MS method was a simple, inexpensive and effective way to measure the volatile compounds in Herba Asari and could be used for the analysis of volatile compounds in complex samples.
- Single-drop micro-extraction,
- Herba Asari,
- Volatile compounds,
- Traditional Chinese medicine
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