Isolation and Electrochemical Property of Tb@C82 Isomers
- Corresponding author: Lian Yongfu, chyflian@hlju.edu.cn
Citation: Dong Wei, Nie Mengsi, Lian Yongfu. Isolation and Electrochemical Property of Tb@C82 Isomers[J]. Acta Chimica Sinica, ;2017, 75(5): 453-456. doi: 10.6023/A17030090
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HPLC conditions: columns: 5PYE, Buckyprep, 5PBB, and Buckyprep-M, Ф 4.6 mm×250 mm; injection volume: 20 μL; eluent: toluene with flow rate of 1 mL/min; detection wavelength: 290 nm at 298 K
(a) Tb@C82 (Ⅰ), (b) Tb@C82 (Ⅱ). Conditions: working electrode, Pt wire; counter electrode, Pt wire; reference electrode, Ag/AgCl; supporting electrolyte, 0.1 mol/L n-Bu4NPF6 in 1, 2-dichlorobenzene; scan rate, 20 mV/s.