Citation: XU Jing, CHEN Min-Dong. Syntheses and Crystal Structures of Complexes Based on 4-[(1H-imidazol-4-yl)methylamino]benzoic Acid Ligand[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(12): 2666-2672. doi: 10.3969/j.issn.1001-4861.2013.00.398
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Reactions of ligand 4-[(1H-imidazol-4-yl)methylamino]benzoic acid (H2L) with transition metal salts led to the formation of three complexes [M(HL)2(H2O)2](M(Ⅱ)=Mn(Ⅱ)(1), Cd(Ⅱ)(2), Cu(Ⅱ)(3)) under different conditions. The single crystal X-ray diffraction analyses revealed that three complexes crystallized in the same triclinic space group P1 are isomorphous and isostructural, and the molecules are further connected by hydrogen bonds interactions resulting in formation of 3D structures. Thermal stability and electrochemistry properties of complexes were also investigated. CCDC: 945340, 1; 945338, 2; 945339, 3.
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-
[1]
[1] Bernstein J, Davey R J, Henck J O. Angew. Chem. Int. Ed., 1999, 38:3441-3461
-
[2]
[2] Eckert H, Ward M. Chem. Mater., 2001, 13:3061-3083
-
[3]
[3] Rao C N R, Natarajan S, Vaidhyanathan R. Angew. Chem. Int. Ed., 2004, 43:1466-1496
-
[4]
[4] Helay F, Maris T, Wuest J D. Cryst. Growth Des., 2008, 8: 4517-4525
-
[5]
[5] Manzano B R, Jaló n F A, Soriano M L, et al. Cryst. Growth Des., 2008, 8:15851594
-
[6]
[6] Li Y P, Yang P. Chin. J. Chem., 2007, 5:1715-1724
-
[7]
[7] Yang X G, Li D S, Fu F, et al. Chin. J. Chem., 2008, 26:655-660
-
[8]
[8] ZHANG Li (张丽), NIU Su-Yun (牛淑云), JIN Jin (金晶), et al. Acta Chim. Sin. (Huaxue Xuebao), 2007, 65:1032-1038
-
[9]
[9] Cote A P, Benin A I, Ockwig N W, et al. Science, 2005, 310: 1166-1170.
-
[10]
[10] Yaghi O M, O′Keeffe M, Ockwig N W, et al. Nature, 2003, 423:705-714
-
[11]
[11] Wu C D, Hu A, Zhang L, et al. J. Am. Chem. Soc., 2005, 127:8940-8941
-
[12]
[12] Fang Q R, Zhu G S, Xue M, et al. Cryst. Growth Des., 2008, 8:319-329
-
[13]
[13] Koh K, Wong-Foy A G, Matzger A J. Angew. Chem. Int. Ed., 2008, 47:677-680.
-
[14]
[14] Song Y, Zhang P, Ren X M, et al. J. Am. Chem. Soc., 2005, 127:3708-3709
-
[15]
[15] Yigit M V, Biyikli K, Moulton B, et al. Cryst. Growth Des., 2006, 6:63-69
-
[16]
[16] Gao H L, Ding B, Yi L, et al. Inorg. Chem. Commun., 2005, 8:151-153
-
[17]
[17] Gao H L, Yi L, Ding B, et al. Inorg. Chem., 2006, 45:481-483
-
[18]
[18] Ghosh S K, Bharadwaj P K. Eur. J. Inorg. Chem., 2005, 4886-4889
-
[19]
[19] Wang H S, Zhao B, Zhai B, et al. Cryst. Growth Des., 2007, 7:1851-1857
-
[20]
[20] Koh C K. Chem. Soc. Rev., 2002, 31:157-167
-
[21]
[21] SAINT, Pragram for Data Extraction and Reduction, Bruker AXS, Inc.; Madison, WI, 2001.
-
[22]
[22] Sheldrick G M. SHELXS-97, Program for Crystal Structure Solution, University of Göttingen, Germany, 1997.
-
[23]
[23] Sheldrick G M. SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.
-
[24]
[24] Hellyer R M, Larsen D S, Brooker S. Eur. J. Inorg. Chem., 2009, 1162-1171
-
[25]
[25] Nicola C D, Garau F, Karabach Y Y, et al. Eur. J. Inorg. Chem., 2009, 666-676
-
[26]
[26] Wang X L, Lin H Y, Liu G C, et al. J. Organomet. Chem., 2008, 693:2767-2774
-
[27]
[27] Wang X L, Zhao H Y, Lin H Y, et al. Electroanalysis, 2008, 20:1055-1059
-
[28]
[28] Younathan J N, Wood K S, Meyer T J. Inorg. Chem., 1992, 31:3280-3285
-
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