Citation: CHEN Man-Sheng, XU Jin-Sheng, DENG Yi-Fang, ZHANG Chun-Hua, KUANG Dai-Zhi, NIE Xue. Hydrothermal Synthesis, Crystal Structure and Photoluminescent Property of Nd(Ⅲ) Complex Constructed from 5-(Isonicotinamido)-isophthalic Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(12): 2673-2677. doi: 10.3969/j.issn.1001-4861.2013.00.390
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The complex [Nd(HINAIP)(INAIP)(H2O)2]n·nH2O was obtained by hydrothermal assembly of Nd(Ⅲ) salt with a 5-(isonicotinamido) isophthalic acid(H2INAIP) and its crystal structure was determined by X-ray single-crystal diffraction. It is of triclinic, P1 space group space group. Single-crystal X-ray diffraction analysis revealed that the HINAIP- and INAIP2- ligands connect Nd(Ⅲ)-carboxylate chains to form 2D layers in complex 1. Finally, It was extended to 3D supramolecular structures by H-bonding interactions. The complex was characterized by TG, IR, UV and near IR fluorescence spectra. CCDC: 958122.
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