Citation: HAO Hong-Qing, CHEN Mu-Hua, LI Xin, PENG Meng-Xia. Structure and Fluorescence of Two Ag(Ⅰ) Complexes Based on 4-Biphenylacetate and 1, 3-Bis(4-pyridyl)propane[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(11): 2480-2484. doi: 10.3969/j.issn.1001-4861.2013.00.370
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Two sandwich-like coordination polymers based on Ag(Ⅰ) and mixed flexible ligands, {[Ag2(bpa)2(bpp)2]·2H2O}n (1) and {[Ag(bpa)(bpp)]·2H2O}n (2) (bpa-=4-biphenylacetate, bpp=1,3-bis(4-pyridyl)propane), have been synthesized by solution reactions of Hbpa, bpp and [Ag(NH3)](OH) with the same ratio under different experimental conditions. They were characterized by single-crystal X-ray diffraction, EA, IRand XRD. Complex 1 is a two-dimensional network based on T-shaped coordination Ag(Ⅰ) ions and Ag…Ag interactions. In 2, the distorted tetrahedral coordination Ag(Ⅰ) ions are further organized by π…π stacking interactions into another two-dimensional network. 1 and 2 exhibit different and intense emissions in the visible region. CCDC: 922168,1;922167, 2.
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