Citation: LI Yun-Tao, HAI Xiao, LIU Xia, ZHANG Ya-Nan. Synthesis, Crystal Structure and Luminescent Property of Zn(Ⅱ) Polymer Coordination Based on 6, 6’-Dithiodinicotinic Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(11): 2475-2479. doi: 10.3969/j.issn.1001-4861.2013.00.355 shu

Synthesis, Crystal Structure and Luminescent Property of Zn(Ⅱ) Polymer Coordination Based on 6, 6’-Dithiodinicotinic Acid

1.
College of Chemistry & Chemical Engineering, Shaanxi University of Science & Techology, Xi'an 710021, China

Received Date: 5 April 2013
Available Online: 5 June 2013
Fund Project: 陕西省科学技术研究中心发展计划项目(No.2012K08-22) (No.2012K08-22)陕西省教育厅科学研究项目计划(No.12JK0627)资助项目 (No.12JK0627)

Anovel zinc coordination polymer {[Zn(cpds)(dpa)]·H₂O}_n (1) (H₂cpds=6,6'-dithiodinicotinic acid, dpa=dipyridin-2-ylamine) has been hydrothermally synthesized and structurally characterized by single-crystal. Complex 1 crystallizes in the triclinic system, space group P1 with a=0.8467(2), b=1.1674(3), c=1.2265(3) nm, α=73.605(3)°, β=78.656(3)°, γ=81.484(3)°, V=1.1347(5) nm³, D_c=1.850 g·cm^-3, Z=2. Single-crystal X-ray analysis reveal that compound 1 contains an infinite 1D chain structure, and the 1D chain was stacked together to form a 3D supramolecular network. Additionally, the fluorescent property and TG analysis for compound 1 were also measured and discussed. CCDC: 931127.
- crystal engineering;coordination polymer;6, 6’-dithiodinicotinic acid;fluerescence
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沈阳化工大学材料科学与工程学院沈阳 110142