Citation: ZUO Luo, FENG Jian-Hua, GUO Li, LI Hui-Hui, WU Gang. Synthesis, Structure, Luminescest and Thermal Stable Properties of 3,4-Pyridinedicarboxylic Acid Barium Complex[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 1979-1984. doi: 10.3969/j.issn.1001-4861.2013.00.291
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Solvothermal reaction of BaCl2·2H2O with 3,4-pyridinedicarboxylic acid afforded a new inorganic-organic hybrid framework,[Ba2(pdc)2(H2O)3]n (1) (H2pdc=3,4-pyridinedicarboxylic acid). This complex has been fully characterized by single crystal X-ray diffraction, elemental analysis, and IR spectrum. X-ray analysis shows that complex 1 features a two-dimensional network (2D). Ba1 takes eight-coordinated distorted square antiprism geometry. Ba2 takes ten-coordinate distorted dicapped square prism coordination geometry. The whole pdc2- anion connects four different Ba(Ⅱ) atoms, giving rise to a 2D network structure. The three-dimensional structure is formed by O-H…N hydrogen bonding interactions. Thermal stability and luminescent property of compound 1 have also been investigated. CCDC: 887479.
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-
[1]
[1] LI Jing(李静), JI Chang-Chun(季长春), WANG Zuo-Wei(王 作为), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2009,25:2083-2089
-
[2]
[2] ZHU Ying-Gui(朱英贵), JU Xue-Hai(居学海), SONG Ying-Lin(宋瑛林), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2008,24(12):2029-2034
-
[3]
[3] Kong C Y. J. Inorg. Organomet. Polym., 2011,21:189-194
-
[4]
[4] Niu C Y, Pan Z L, Dang Y L, et al. J. Inorg. Organomet. Polym., 2011,21:611-618
-
[5]
[5] Baxter P N W, Khoury R G, Lehn J M, et al. Chem. Eur. J., 2000,6:4140-4148
-
[6]
[6] Long D L, Blake A J, Champness N R, et al, Chem. Eur. J., 2002,8:2026-2033
-
[7]
[7] Su C Y, Cai Y P, Chen C L, et al. J. Am. Chem. Soc., 2003, 125:8595-8613
-
[8]
[8] Ciurtin D M, Pschirer N G, Smith M D, et al. Chem. Mater., 2001,13:2743-2745
-
[9]
[9] Baxter P N W, Lehn J M, Baum G, et al. Chem. Eur. J., 2000,6:4510-4517
-
[10]
[10] Pan L, Huang X Y, Li J, et al. Angew. Chem., Int. Ed., 2000,39:527-530
-
[11]
[11] Abuhmaiera R, Lan Y, Ako A M, et al. CrystEngComm, 2009,11:1089-1096
-
[12]
[12] Motreff A, da Costa R C, Allouchi H, et al. Inorg. Chem., 2009,48:5623-5625
-
[13]
[13] Berggren G, Anderlund M F, Styring S, et al. Inorg. Chem., 2012,51:2332-2337
-
[14]
[14] Bo Q B, Sun Z X, Song G L, et al. J. Inorg. Organomet. Polym., 2007,17:615-622
-
[15]
[15] Wang F, Liu Z S, Yang H, et al. Angew. Chem., Int. Ed., 2011,50:450-453
-
[16]
[16] Cao R, Lu J, Batten S R, CrystEngComm, 2008,10:784-789
-
[17]
[17] Zhang X, Huang Y Y, Zhang M J, et al. Cryst. Growth Des., 2012,12:3231-3238
-
[18]
[18] Sheldrick G M. SHELXS 97, Program for the Solution of Crystal Structure, University of Göttingen, Germany, 1997.
-
[19]
[19] Sheldrick G M. SHELXL 97, Program for the Refinement of Crystal Structure, University of Göttingen, Germany, 1997.
-
[20]
[20] Fromma K M, Goesmann H. Acta Cryst. C56, 2000:1179-1180
-
[21]
[21] Yu J O, Cté A P, Enright G D, et al. Inorg. Chem., 2001,40: 582-583
-
[22]
[22] Zhu H F, Zhang Z H, Sun W Y, et al. Cryst. Growth Des., 2005,5:177-182
-
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