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Citation: GUO Li-Fang, WANG Zhao-Xi, LI Ming-Xing. A Two-Dimensional Manganese(Ⅲ) Coordination Polymer Constructed from[Mn3O] Units：Synthesis, Crystal Structure and Magnetic Properties[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 1921-1927. doi: 10.3969/j.issn.1001-4861.2013.00.274 shu

A Two-Dimensional Manganese(Ⅲ) Coordination Polymer Constructed from[Mn3O] Units：Synthesis, Crystal Structure and Magnetic Properties

  • 1.

    1 Department of Chemistry, College of Science, Shanghai University, Shanghai 200444, China;

  • Received Date: 1 February 2013
    Available Online: 1 May 2013

    Fund Project: 国家自然科学基金(No.20901049, 21171115) (No.20901049, 21171115)浙江省有机化学与皮革化工重中之重学科开放基金(No.100061200130)资助项目。 (No.100061200130)

  • A 2D coordination polymer, namely {[NaMn3ⅢO(sao)3(tfbdc)(H2O)4]·0.5H2O·2CH3CH2OH}n(1) (H2tfbdc=2, 3, 5, 6-tetrafluoroterephthalic acid, H2sao=salicylaldoxime), was synthesized and structurally characterized by elemental analysis, IR spectrum, thermogravimetric analysis, and single-crystal X-ray diffraction. This complex crystallizes in triclinic space group P1, and exhibits a two-dimensional polymeric structure constructing from[Mn3O] units bridged by sodium cations and tetrafluoroterephthalate. Variable-temperature magnetic susceptibility analysis indicates that antiferromagnetic interaction exists between the manganese(Ⅲ)ions in the[Mn3O] unit. CCDC: 934761.
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