Citation: KONG Zhi-Guo, SUN Xu-Ran, LI He, FAN Yan-Jia, ZHANG Lin. Synthesis, Structure and Characterization of Pb(Ⅱ) Coordination Polymer Constructed by 1,10-Phenanthroline Derivative and Succinic Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 1942-1946. doi: 10.3969/j.issn.1001-4861.2013.00.249
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A coordination polymer,[Pb2(L1)2(L2)2] (1) (H2L1=succinic acid and L2=2-(4-fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline), has been hydrothermally synthesized and characterized by elemental analysis, IR spectroscopy, TGA and single-crystal X-ray diffraction. Crystal data: C46H30F2N8O8Pb2, monoclinic, space group P21/c, a=0.795 40(10) nm, b=2.649 0(3) nm, c=1.996 9(2) nm, β=99.784(2)°, V=4.146 3(9) nm3, Z=4, R=0.038 0, wR=0.0845. In 1, each L1 anion in a bis-chelating mode bridges Pb(Ⅱ) atoms to afford a one-dimensional (1D) chain structure. Neighboring 1D chains are linked together by π-π stackings among L2 ligands to yield a 3D supramolecular architecture. Finally, the N-H…O hydrogen-bonding interactions further stabilize the 3D supramolecular structure of 1.
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