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Citation: ZHANG Qing, LIU Chun-Bo, CHE Guang-Bo, WANG Shi-Meng, BAI Hong-Ye, SHI Fa-Nian. Hydrothermal Synthesis and Crystal Structure of a Two Dimensional Pb(Ⅱ) Complex Based on 2-(2-Carboxyphenyl)-1H-imidazo[4,5-f][1,10]phenanthroline[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(10): 2183-2187. doi: 10.3969/j.issn.1001-4861.2013.00.242 shu

Hydrothermal Synthesis and Crystal Structure of a Two Dimensional Pb(Ⅱ) Complex Based on 2-(2-Carboxyphenyl)-1H-imidazo[4,5-f][1,10]phenanthroline

  • 1.

    1 School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang, Jiangsu 212013, China;

  • Received Date: 23 October 2012
    Available Online: 11 March 2013

    Fund Project: 江苏大学自然科学基金(No.09JDG001,No.11jdg104)资助项目 (No.09JDG001,No.11jdg104)

  • Acoordination polymer, [PbL2]n (1) (HL=2-(2-carboxyphenyl)-1H-imidazo[4,5-f][1,10]phenanthroline) has been hydrothermally synthesized and characterized by IRspectrum, elemental analysis and X-ray single-crystal diffraction. Complex 1 crystallizes in monoclinic, space group P21/c with a=1.34585(9) nm, b=0.70943(5) nm, c=3.2655(2) nm, β=99.6260(10)°, V=3.0740(4) nm3, Z=4, C40H22N8O4Pb, Mr=885.85, Dc=1.914 g·cm-3, μ(Mo Kα)=5.551 mm-1, F(000)=1728, GOOF=1.038, the final R=0.0270 and wR=0.0581 for 5067 observed reflections (I>2σ(I)). Structural analysis shows that the complex 1 presents a two dimensional layer structure. Thermal stability and luminescent property were also investigated. CCDC: 900402.
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