Citation: MA Zhi-Hong, WANG Na, GUO Kai-Ming, LIN Jin, ZHENG Xue-Zhong. Synthesis and Structures of Substituted Tetramethylcyclopentadienyl Diruthenium Complexes[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 1882-1886. doi: 10.3969/j.issn.1001-4861.2013.00.237
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The ligands[C5Me4HR] (R=cyclopentyl,cyclohexyl,nPr) reacted with Ru3(CO)12 in refluxing xylene to give three new substituted tetramethylcyclopentadienyl diruthenium metal carbonyl complexes[(η5-C5Me4R)Ru(CO)(μ-CO)]2 (R=cyclopentyl (1),cyclohexyl (2),nPr (3)),respectively. The three new complexes were characterized by IR,elemental analysis and 1H NMR spectra. The crystal structure of complexes 1 and 2 was determined by X-ray single crystal diffraction. CCDC: 891140, 1; 837727, 2.
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